DRINKING WATER
Analysis

Minimum Volume

Container Type

Required Preservative

Holding Time from Date/Time Sampled

Coliform, Total/E. Coli

Volatile Organics by 524.2 Volatile Organics


Trihalomethanes (THM)

Metals
Alkalinity


Chloride
Color
Fluoride, total
pH
Nitrate


Nitrite
Sulfate
Turbidity
Conductivity
Chlorine Residual
Odor
Hardness
100ml

2 X 40 ML



2 X 40 ML

1 liter
250ml


250ml
250ml
250ml
250ml
250ml


250ml
250ml
250ml
250ml
250ml
250ml
250ml
Sterile, plastic

Vials with Teflon lined septum


Vials with Teflon lined septum
Plastic
Plastic


Plastic
Plastic
Plastic
Plastic
Plastic


Plastic
Plastic
Plastic
Plastic
Plastic
Plastic
Plastic
0.008% Na2S2O3

Ascorbic acid (25mg/40ml) added to empty sample bottle then add 1:1 HCL to pH<2. Cool 4ºC
0.008%Na2S2O3

HNO3 to pH<2
Separate Bottle completely filled to the exclusion of air. Cool 4ºC
None
Cool 4ºC
None
None
Cool 4ºC


Cool 4ºC
Cool 4ºC
Cool 4ºC
Cool 4ºC
Cool 4ºC
Cool 4ºC
HNO3 to pH<2
8 hours surface water and 30 hours fully processed drinking water
Analysis: 14 Days



Analysis: 14 Days

Analysis: 6 months
Analysis: 14 Days


Analysis: 28 Days
Analysis: 48 hours
Analysis: 28 Days
Analysis: 1 hour
Analysis: By IC: 48 hours Chlorinated Supplies: 14 days Non-chlorinated Supplies: 28 days
Analysis:48 hours
Analysis: 28 days
Analysis: 48 hours
Analysis: 28 Days
Analysis: 15 min
Analysis: 24 hours
Analysis: 6 months


NON-POTABLE WATER
Analysis

Minimum Volume

Container Type

Required Preservative

Holding Time from Date/Time Sampled

Semi-volatile Organics by EPA 625 or EPA 8270C

Volatile Organics by EPA 624 or EPA 8260B
Metals by EPA 200.7
Hardness
Pesticides by EPA 608

PCB’s by EPA 608

Mercury by EPA 7470A
Cyanide by EPA 9014

Chromium VI by EPA 7196A
1000ml


3 X 40 ML

1000ml
250ml
1000ml

1000ml

250ml
250ml

500ml
Glass, Teflon-lined cap


Vials with Teflon lined septum
Plastic
Plastic
Glass, Teflon-lined cap

Glass, Teflon-lined cap

Plastic
Plastic

Plastic
Cool to ≤ 6ºC, 0.008% Na2S2O3 for residual chlorine only, store in dark
Ascorbic acid (25mg/40ml) for residual chlorine
HNO3 to pH<2
H2SO4 to pH<2
Cool to ≤ 6ºC, pH 5-9, 0.0008% Na2S2O3 for residual chlorine
Cool to ≤ 6ºC

HNO3 to pH <2
Cool to ≤ 6ºC NaOH to pH >12, 0.6g, no sulfide
Cool to ≤ 6ºC plus pH 9.3-9.7 with (NH4)2SO4
7 days until extraction
40 days after extraction to analysis

Analysis: 14 Days (7 days if not preserved)

Analysis: 6 months
Analysis: 6 months
72 hours 7 days until extraction 40 days after extraction to analysis
1 year to extraction and 1 year after extraction for analysis
Analysis: 28 days
Analysis: 48 hours 14 Days

Analysis: 24 hours 28 days


SOLID AND HAZARDOUS WASTE
Analysis

Minimum Volume

Container Type

Required Preservative

Holding Time from Date/Time Sampled

BNA by EPA 8270C

Cyanide by EPA 9014

DRO by EPA 8015

GRO by EPA 8015

Herbicides by 8151A

Lead in Paint
Mercury by EPA 7471A

Metals

PCBs by EPA 8082

Pesticides by EPA 8081A

Volatile Organics by
EPA 8260B
Cyanide by EPA 9014

Chromium by EPA 7196A
250ml wide mouth container
250ml wide mouth container
250ml wide mouth container
250ml wide mouth container
250ml wide mouth container
5g
250ml wide mouth container
250ml wide mouth container
250ml wide mouth container
250ml wide mouth container
250ml wide mouth container or 2 x40ml vial
250ml wide mouth container
250ml wide mouth container
Glass , Teflon-lined cap

Plastic

Glass, Teflon lined cap

Glass, Teflon lined cap

Glass, Teflon-lined cap

Plastic
Plastic

Plastic

Glass, Teflon-lined cap

Glass, Teflon-lined cap

Glass, Teflon lined cap

Plastic

Plastic
Cool 6ºC

None

Cool 6ºC

Cool 6ºC

Cool 6ºC

None
None

None

Cool 6ºC

Cool 6ºC

Cool 6ºC

Cool 6ºC

Cool 6ºC
14 days until extraction 40 days after extraction to completion of analysis
Analysis: 14 Days

Analysis: 7 days

Analysis: 7 days

14 days until extraction 40 days after extraction to completion of analysis
Not listed
Analysis: 6 months

Analysis: 6 months

14 days until extraction 40 days after extraction to completion of analysis
14 days until extraction 40 days after extraction to completion of analysis
Analysis: 14 days

Anaylsis: 48 hours

Analysis: 24 hours


CTDOH STANDARD PROFILE
Analysis

Minimum Volume

Container Type

Required Preservative

Holding Time from Date/Time Sampled

Coliform, Total/E. Coli

Metals – Iron, Manganese, Sodium
Chloride
Color
pH
Nitrate


Nitrite
Sulfate
Turbidity
Chlorine Residual
Odor
Hardness
100ml

1 liter

250ml
250ml
250ml
250ml


250ml
250ml
250ml
250ml
250ml
250ml
Sterile, plastic

Plastic

Plastic
Plastic
Plastic
Plastic


Plastic
Plastic
Plastic
Plastic
Plastic
Plastic
0.008% Na2S2O3

HNO3 to pH<2

None
Cool 4ºC
None
Cool 4ºC


Cool 4ºC
Cool 4ºC
Cool 4ºC
Cool 4ºC
Cool 4ºC
HNO3 to pH<2
8 hours surface water and 30 hours fully processed drinking water
Analysis: 6 months

Analysis: 28 Days
Analysis: 48 hours
Analysis: 1 hour
Analysis: By IC: 48 hours Chlorinated Supplies: 14 days Non-chlorinated Supplies: 28 days
Analysis: 48 hours
Analysis: 28 days
Analysis: 48 hours
Analysis: 15 min
Analysis: 24 hours
Analysis: 6 months